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Size shrinkage and compressive behaviour of Al2O3 honeycomb structures fabricated via Digital Light Processing technology

CERAMICS INTERNATIONAL [2024]
Yangli Xu, Zeling Yang, Guoqin Huang, Chenxu Ren, Guangyao Han, Xiaopeng Jiang, Tingting Li, Congming Ke, Yong Zeng, Xipeng Xu
ABSTRACT

Al 2 O 3 ceramic have excellent chemical inertness, superior heat resistance, and excellent corrosion resistance, so they are considered ideal materials for manufacturing high-performance components such as thermal end devices in aerospace, heat dissipation panels in electronic communication, and exhaust filters in the automotive industry. Digital Light Processing (DLP) is a useful technology to fabricate complex Al 2 O 3 ceramic components. However, the size shrinkage effect of DLP-fabricated components need to be investigated deeply before its further application. In this work, we utilized DLP technology to fabricate Al 2 O 3 ceramic honeycomb structures and systematically investigated their microstructure, size shrinkage, and mechanical properties. Our findings revealed that the Al 2 O 3 ceramic grains exhibit flake-like structures with an average diameter of 1–2 μm, and the ceramic particles are tightly bonded. The shrinkage rates in the X and Y axes were 7.54 % and 7.42 %, respectively, while the Z-axis exhibited a more significant shrinkage of 13.04 %. This anisotropic shrinkage in different direction was attributed to accumulation of the interlayer bonding under gravity action during debinding and sintering process. The compressive stress-strain curve of the honeycomb structures demonstrated a typical brittle compressive behavior, including elastic, stress plateau, and brittle fracture stages. The honeycomb structures exhibited an elastic modulus of 54.49 ± 1.22 MPa and a compressive strength of 10.22 ± 0.42 MPa. The fracture analysis indicated that the fractures region of honeycomb structures initiated at the corners of the honeycomb structures, indicating their easy-broken compared to the walls. These findings provide valuable guidance for the high-precision and high-performance manufacturing of complex Al 2 O 3 ceramic components.

MATERIALS

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