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Protocol for the preparation and application of CeO2-CuO catalysts in the decarboxylative oxidation reaction of benzoic acids to phenols

STAR Protocols [2024]
Xinze Du, Yumei Liu, Xiaojun Shen
ABSTRACT

Summary Phenolic chemicals are important building blocks in chemical and material industries. In this protocol, we describe the preparation of CeO 2 -CuO catalysts and the application in the decarboxylative oxidation reaction of benzoic acids to phenols. Furthermore, we describe how to modify the basic sites of CeO 2 -CuO catalysts by CO 2 treatment to increase the selectivity of phenol and the regeneration process of used catalyst. For complete details on the use and execution of this protocol, please refer to Du et al. (2023). 1

MATERIALS

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