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The effect of phosphate/TiO2 composite insulating layer on the high frequency magnetic properties of FeSiBPCNbCu nanocrystalline soft magnetic powder cores

Materials Today Communications [2024]
Junyao Zhang, Yaqiang Dong, Yanqiu Li, Liping Yang, Xingjie Jia, Ling Zhang, Lingwen Cai, Aina He, Jiawei Li, Xincai Liu, Baogen Shen
ABSTRACT

Currently, power electronic devices are developing to meet the requirement of miniaturization, high-frequency and low-power consumption, reducing the high-frequency loss of soft magnetic powder cores (SMPCs) is one of the popular research topics. The construction of multilayer insulating structures can reduce the core loss ( P cv ) of SMPCs by increasing the resistivity. In this work, a composite inorganic insulating layer of phosphate and TiO 2 was successfully synthesized on the powder surface by phosphating and then sol-gel method. At last a nanocrystaline SMPCs with excellent soft magnetic properties were prepared with epoxy resin as the binder. The cores were heat-treated at 510 ℃ for 1 h to achieve optimum soft magnetic properties, with a low P cv of 854 mW/cm 3 at 20 mT and 2 MHz, an effective permeability ( μ e ) of 40 at 10 MHz and excellent DC bias with a percent permeability of 74% of the initial value at 100 Oe. The synergistic effect of the epoxy - TiO 2 - phosphate - nanocrystalline powder multilayer interface effectively reduces inter-particle eddy current loss, resulting in a significant reduction in the P cv of the SMPCs.

MATERIALS

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